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酸性染料用固色剂的合成及应用

王丽 周向东 史亚鹏 张海玲

印染助剂2012,Vol.29Issue(4):18-22,5.
印染助剂2012,Vol.29Issue(4):18-22,5.

酸性染料用固色剂的合成及应用

Synthesis and application of a fixing agent applied to acid dyes

王丽 1周向东 2史亚鹏 1张海玲2

作者信息

  • 1. 苏州大学现代丝绸国家工程实验室,江苏苏州215123
  • 2. 苏州大学纺织与服装工程学院,江苏苏州215021
  • 折叠

摘要

Abstract

A fixing agent SBNF with sulfonic group for acid dyes was synthesized using bisphenol A, 2-naphthol, formaldehyde as the main raw materials. The influences of reactant mass ration, reaction time and temperature, the dosage of fixing agent, fixing time, pH of fixing solution on the fixation effect were discussed. The synthesis process and application technology were optimized and the optimum synthetic process was as follows: mfsulfonation intermediate Ⅰ ):m(sulfonation intermediate Ⅱ):m(formaldehyde)=2.0 :1.0:1.0, reacted at 100 ℃ for 6 h; and the optimal application technology was: 2.5% (owf) of SBNF fixing agent, 10% (owf) of formaldehyde scavenger, pH=3.0, fixed acid dyed polyamide fabric at 80 ℃ for 30 min. The fixed fabric had fairly good color fastness, such as 3~4-level to wet rubbing, 4-level to dry rubbing and 4-level to soaping.

关键词

酸性染料/固色剂/合成/应用

Key words

acid dyes/ fixing agent/ synthesis/ application

分类

化学化工

引用本文复制引用

王丽,周向东,史亚鹏,张海玲..酸性染料用固色剂的合成及应用[J].印染助剂,2012,29(4):18-22,5.

基金项目

江苏高校优势学科建设工程资助项目(PAPD) (PAPD)

印染助剂

OA北大核心CSTPCD

1004-0439

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