安徽农业科学Issue(12)：7135-7136,2.
2-(4-硝基苯基)苯并咪唑的合成
Synthesis of 2-(4- Nitrylphenyl) Benzimidazole
摘要
Abstract
The easy way for para-nitrobenzaldehyde and o-phenylenediamine to be directly synthesized into 2-(4-nitrylphenyi) benzimidazole was studied, and the structure of target product was analyzed by melting point detector, elementary analyzer and infrared spectrum. As indicated by the results, when the molar ratio of o-phenylenediamine to para-nitrobenzaldehyde was 1:1.4, the reaction time was 3 h, and the temperature was 65℃, the yield of products could reach 70. 14%. The experiment was repeated under the same conditions, the yield was above 70.0%. The products obtained through this method had the advantages of good color, easy posttreatment and little corrosion to equipment, proving that the method had high application value.关键词
苯并咪唑/对硝基苯甲醛/邻苯二胺/合成Key words
Benzimidazole/ P-nitrobenzaldehyde/ O-phenylenediamin/ Synthesis分类
农业科技引用本文复制引用
于丽颖,罗亚楠,方圆..2-(4-硝基苯基)苯并咪唑的合成[J].安徽农业科学,2012,(12):7135-7136,2.基金项目
吉林省教育厅科研项目(2010NO176). （2010NO176）
