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首页|期刊导航|聊城大学学报:自然科学版|焙烧温度对二氧化硅负载磷钼酸铵催化剂苯硝化活性的影响

焙烧温度对二氧化硅负载磷钼酸铵催化剂苯硝化活性的影响

刘丽君 张俊玲 唐叶 陶绪泉 张海波

聊城大学学报:自然科学版2012,Vol.25Issue(2):52-55,4.
聊城大学学报:自然科学版2012,Vol.25Issue(2):52-55,4.

焙烧温度对二氧化硅负载磷钼酸铵催化剂苯硝化活性的影响

Effect of the Calcination Temperature on the Catalytic Activity of Silica Supported Ammonium Molybdophosphat Catalyst for Benzene Nitration

刘丽君 1张俊玲 1唐叶 1陶绪泉 2张海波3

作者信息

  • 1. 聊城大学化学化工学院,山东聊城252059
  • 2. 聊城大学材料科学与工程学院,山东聊城252059
  • 3. 山东昌裕集团聊城齐鲁漆业有限公司,山东聊城252036
  • 折叠

摘要

Abstract

After drying and calcination, silica supported ammonium molybdophosphat catalyst was prepared by sol-gel method with ethyl orthosilicate as silica source. And the catalyst was characterized by X-ray diffraction(XRD), IR spectra and the potentiometric titration method, as well as the catalytic activity of catalyst in nitration of benzene was tested. Results indicated that calcination temperature had obvious influence on the catalytic reaction, and the catalyst that calcinated at 300℃ exhibited excellent catalytic activity and stability.

关键词

二氧化硅/焙烧温度/催化//硝化

Key words

silica/calcination temperature/catalysis/benzene/nitration

分类

化学化工

引用本文复制引用

刘丽君,张俊玲,唐叶,陶绪泉,张海波..焙烧温度对二氧化硅负载磷钼酸铵催化剂苯硝化活性的影响[J].聊城大学学报:自然科学版,2012,25(2):52-55,4.

基金项目

聊城大学大学生科技文化创新基金项目 ()

聊城大学学报:自然科学版

OACHSSCD

1672-6634

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