同济大学学报（自然科学版）2012，Vol.40Issue(5)：779-782,788,5.DOI:10.3969/j.issn.0253-374x.2012.05.024
丝氨酸铋(Ⅲ)配合物的固相合成与表征
Solid Phase Synthesis and Characterization of Serine Complex of Bismuth(Ⅲ)
摘要
Abstract
New serine complex of bismuth (Ⅲ), (C3H6O3N)2Bi(μ-I)2Bi[(C3H8OiN)I] ? H2O was synthesized by the solid phase reaction at room temperature. The complex has been characterized by elemental analysis. X-ray powder diffraction, far-infrared spectra and TG-DTA analysis. The results of indexing of the X-ray diffraction patterns indicate the crystal structure of bismuth complex with serine belongs to a orthorhombic system and the lattice parameters are:a= 0.796 7 nm. 6=1.987 5 nm, c=2.203 4 nm.关键词
丝氨酸/铋(Ⅲ)/配合物/固相合成Key words
serine/ bismuth (Ⅲ)/complexi solid phase synthesis分类
通用工业技术引用本文复制引用
杨宇翔,纪国媛,林海,刘昌立..丝氨酸铋(Ⅲ)配合物的固相合成与表征[J].同济大学学报（自然科学版）,2012,40(5):779-782,788,5.基金项目
温州市科技计划项目(G20100173) （G20100173）
吉林大学无机合成与制备化学国家重点实验室项目(2011-30) （2011-30）
