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荻原料烧碱-蒽醌法蒸煮过程中甲醇发生量的研究

闫晓峰 刘秋娟

天津科技大学学报2012,Vol.27Issue(3):29-32,4.
天津科技大学学报2012,Vol.27Issue(3):29-32,4.

荻原料烧碱-蒽醌法蒸煮过程中甲醇发生量的研究

Study of Methanol Formation During Soda-AQ Cooking Process of Silver Grass

闫晓峰 1刘秋娟1

作者信息

  • 1. 天津市制浆造纸重点实验室,天津科技大学材料科学与化学工程学院,天津300457
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摘要

Abstract

Methanol formation during soda-AQ cooking process of Silver grass was investigated by using the headspace chromatography(HSGC). The formation regulations of methanol in different cooking conditions with different alkali charge, cooking temperature and holding time were also studied. The results showed that alkali charge,holding time and cooking temperature all had great influence on the methanol formation. With the increase of the alkali charge, holding time and cooking temperature, the amount of the methanol formation increased rapidly. When the alkali charge increased from 10% to 20%, the generated methanol changed from 2.34 kg/t(odp)to 5.06 kg/t(odp). When the holding time extended from 10 min to 40 min.the generated methanol changed from 2.08 kg/t(odp)to 3.88 kg/t(odp). When the cooking temperature increased from 145 ℃ to 170 ℃, the amount of the methanol varied from 2.02 kg/t (odp) to 4.37 kg/t(odp). But the heating up time has a relatively small effect on the amount of methanol formation.

关键词

/顶空气相色谱/甲醇发生量

Key words

Silver grass/ GCHS/ methanol formation

分类

轻工纺织

引用本文复制引用

闫晓峰,刘秋娟..荻原料烧碱-蒽醌法蒸煮过程中甲醇发生量的研究[J].天津科技大学学报,2012,27(3):29-32,4.

基金项目

国家自然科学基金资助项目(21077076) (21077076)

天津科技大学学报

1672-6510

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