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GC-MS法检测化妆品中6种邻苯二甲酸酯

董伟峰 徐杨 陈溪 白翎 牟明仁 张翠芬

大连工业大学学报2012,Vol.31Issue(4):265-267,3.
大连工业大学学报2012,Vol.31Issue(4):265-267,3.

GC-MS法检测化妆品中6种邻苯二甲酸酯

Determination of 6 kinds of phthalate acid esters in cosmetics by GC-MS

董伟峰 1徐杨 1陈溪 2白翎 1牟明仁 1张翠芬3

作者信息

  • 1. 辽宁出入境检验检疫局,辽宁大连 116001
  • 2. 大连出入境检验检疫局,辽宁大连 116400
  • 3. 大成食品有限公司,辽宁大连 116308
  • 折叠

摘要

Abstract

Gas chromatography-mass spectrometry (GC-MS) technology was used to detect six kinds of phthalic acid esters (DMP, DEP, DBP, BBP, DEHP, DNOP) in the solid, semi-solid and liquid of cosmetics. The sample was detected after extraction by methyl alcohol and dehydration by anhydrous sodium sulfate, in which the method detection limit was 0. 2 mg/kg, the average recovery was 71. 7% to 109. 0%, the average relative standard deviation (RSD) was 1. 57%-4. 53%. The method can meet detection of 6 phthalate esters in all kinds of cosmetics.

关键词

化妆品/邻苯二甲酸酯/气相色谱-质谱分析

Key words

cosmetics/ phthalic acid esters/ gas chromatography-mass spectrometry

分类

轻工纺织

引用本文复制引用

董伟峰,徐杨,陈溪,白翎,牟明仁,张翠芬..GC-MS法检测化妆品中6种邻苯二甲酸酯[J].大连工业大学学报,2012,31(4):265-267,3.

大连工业大学学报

OA北大核心CSTPCD

1674-1404

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