广东药学院学报2012,Vol.28Issue(3):287-290,4.DOI:10.3969/j.issn.1006-8783.2012.03.014
檀香叶的HPLC指纹图谱研究
Study on the fingerprint of the leaves of Santalum album with HPLC
摘要
Abstract
Guangdong Zhanjiang Testing Base for South Medical Materials .Zhanjiang 524338, China Objective To establish the HPLC fingerprint of leaf of Santalum album. Methods The separation was achieved on a C18 column(5 μm,250 mm ×4.6 mm,Agilent) with a mobile phase consisting of methanol-0.5% acetic acid,with gradient elution. The flow rate was 1 mL/min. The detection wavelength was at 338 nm,and column temperature was maintained at 30 ℃. Results Ten batches of the leaves of Santalum album were determined,and 13 common peaks were identified with a good separation. The similarity between various samples and the automatically generated reference fingerprints reached above 0.94. Conclusion The method is simple and effective for control the quality of leaves of Santalum album.关键词
檀香叶/指纹图谱/高效液相色谱法Key words
leaf of Santalum album/ fingerprint/ HPLC分类
中医学引用本文复制引用
闫冲,林励,徐道华,蔡聪,郑来安,王伟梅..檀香叶的HPLC指纹图谱研究[J].广东药学院学报,2012,28(3):287-290,4.基金项目
教育部博士点基金项目(20094425110009) (20094425110009)
广东高校优秀青年创新人才计划培养项目 ()
广东省大学生创新实验项目(KY1026) (KY1026)