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火锅飘香剂挥发性成分的气相色谱-质谱法研究

潘政春 路宁维 安琼 董钰明

兰州大学学报(医学版)2012,Vol.38Issue(2):22-25,4.
兰州大学学报(医学版)2012,Vol.38Issue(2):22-25,4.

火锅飘香剂挥发性成分的气相色谱-质谱法研究

Study of the volatile components of the hotpot flavors additive from gas chromatography-mass spectrometry

潘政春 1路宁维 2安琼 1董钰明1

作者信息

  • 1. 兰州大学药学院,甘肃兰州730000
  • 2. 江苏豪森医药研究院,江苏连云港222002
  • 折叠

摘要

Abstract

Objective To study the composition of the volatile components in the hotpot flavors additive and to establish a fast and accurate method for the quality control of the hotpot flavors additive. Methods The sample was dissolved with the methylene chloride and injected into gas chromatography-mass spectrometer with the split mode. The peaks were identified by manual and comparison spectra. The relative percentage contents of each volatile component were determined by spectrum peak normalization. Results Forty possible volatile components were separated in the hotpot flavors additive and twenty-one of them were identified. The identified constituents were about 19.88% of the total volatile components. The major constituents were ketenes, alcohols, fats, steroids compounds. Conclusion The established method is a rapid approach for separation and identification of the volatile components in the hotpot flavors additive and it can be used as an. alternative method for the quality control of the hotpot flavors additive.

关键词

火锅飘香剂/挥发性成分/气相色谱-质谱法

Key words

hotpot flavors additive/ volatile components/ gas chromatography-mass spectrometry

分类

医药卫生

引用本文复制引用

潘政春,路宁维,安琼,董钰明..火锅飘香剂挥发性成分的气相色谱-质谱法研究[J].兰州大学学报(医学版),2012,38(2):22-25,4.

基金项目

兰州大学中央高校基本科研业务费专项基金(lzujbky-2011-93) (lzujbky-2011-93)

兰州大学学报(医学版)

OACSTPCD

1000-2812

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