人工晶体学报2012，Vol.41Issue(3)：708-713,6.
溶剂热合成球形Cu2ZnSnS4(CZTS)微粉的研究
Research on Synthesis of Spherical Cu2ZnSnS4 ( CZTS) Micropowder by Solvothermal Method
摘要
Abstract
Cu2ZnSnS4 (CZTS) powder were successfully synthesized by high pressure solvothermal route. The synthesis products'phase and morphology of the as-synthesized products were investigated by X-ray diffraction (XRD) and Scanning Electron Microscope (SEM). The influence of synthetic conditions Buch as temperature, synthetic time and dispersant on the phase and morphology of the sphere-like CZTS particles were studied. The results showed that pure sphere-like CZTS particles composed of tiny thin flakes were obtained by high pressure solvothermal route in short time, the reaction process was accelerated with increasing temperatures, and the products were completed with increasing holding time. The surface active agent used plays a less significant role in the synthesis process.关键词
溶剂热/CZTS/球形微粉Key words
solvothermal route/ CZTS/ sphere-like particles分类
信息技术与安全科学引用本文复制引用
邹正光,曾彦,龙飞,申玉芳,郑国源..溶剂热合成球形Cu2ZnSnS4(CZTS)微粉的研究[J].人工晶体学报,2012,41(3):708-713,6.基金项目
国家自然科学基金(51162005,50902024) （51162005,50902024）
广西高校优秀人才资助计划项目(桂教人[2011]40号) （桂教人[2011]40号）
