铀矿地质2012，Vol.28Issue(3)：165-172,180,9.DOI:10.3969/j.issn.1000-0658.2012.03.007
镍箔恒温自沉积总α、总β计数法同时或连续测定样品中210pb、210Bi、210po
The Determination of 210Pb, 210Bi, 210Po by Counting Gross α and Gross β Rate of Spontaneous Deposited Samples on Ni Foil
王玉学 1郭冬发 2黄秋红1
作者信息
- 1. 核工业北京地质研究院,北京100029
- 2. 核工业240研究所,辽宁沈阳110032
- 折叠
摘要
Abstract
Uncertainty evaluation on the criteria of "ferrous sulfate deoxidization / ammonium vanadate oxidation titrimetry to measure uranium" (EJ267.2-84) issued by Ministry of Nuclear Industry was analyzed. The uncertainty brought by the method itself was obtained through the identification of uncertainty sources, quantification of uncertainty components and determination of uranium content by titration with calibrated ammonium vanadate solution. With the analytical study to uncertainty sources of entire process and components, and the application of statistical treatment based on scientific data, the combined standard uncertainty and expanded uncertainty about different levels of uranium content was reported.关键词
210Pb/210Bi/210Po/同时测定/连续测定Key words
uncertainty/ uranium/ volumetry/evaluation分类
天文与地球科学引用本文复制引用
王玉学,郭冬发,黄秋红..镍箔恒温自沉积总α、总β计数法同时或连续测定样品中210pb、210Bi、210po[J].铀矿地质,2012,28(3):165-172,180,9.
