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GC-MS测定姜油中α-蒎烯·桉油精和龙脑的含量

马雯芳 谭建宁 徐东来 严克剑

安徽农业科学2012,Vol.40Issue(21):11030-11031,11116,3.
安徽农业科学2012,Vol.40Issue(21):11030-11031,11116,3.

GC-MS测定姜油中α-蒎烯·桉油精和龙脑的含量

Determination of α-pinene, Eucalyptol and Borneol in Volatile Oil from Zingiber officinale Roscoe by GC-MS

马雯芳 1谭建宁 1徐东来 2严克剑3

作者信息

  • 1. 广西中医药大学药学院,广西南宁530001
  • 2. 广西壮族自治区南宁食品药品检验所,广西南宁530001
  • 3. 广西中医药研究院,广西南宁530022
  • 折叠

摘要

Abstract

[ Objective] To establish a method for determination of a-pinene, euealyptol and boireol in volatiJe oil from Zingiber officinnle Roscoe by GC-MS. [ Method] Contents of a-pinene, eucalyptoi and faomeol in volatile oil from Zingiber officinale Roacoe were determined by GC-MS. [Result] The luiearity of o-pinene, eucalyptol and bomeol were shown in the range of 20.01 -300.15 礸/ml (r = 0.999 5), 34. 74 -521.10 礸/ml (r = 0.999 0) and6.48 -97.20 礸/ml (r =0.999 5). The average recovery rate of a-pinene, eucalyptol and bomeol were 101. 09% with RSD of 1. 35% , 97.78% with RSD of 1. 86% , and 103. 28% with RSD of 1.57 % (n = 6) respectively. [ Conclusion ] The determination method is sensitive, rapid and accurate, it could be user! as the determination method for Zingiber offwirwle Roscoe.

关键词

姜油/α-蒎烯/桉油精/龙脑/GC-MS/含量测定

Key words

Volatile oil/ a-pinene/ Eucalyptol/ Bonieol/ GC-MS/ Content determination

分类

农业科技

引用本文复制引用

马雯芳,谭建宁,徐东来,严克剑..GC-MS测定姜油中α-蒎烯·桉油精和龙脑的含量[J].安徽农业科学,2012,40(21):11030-11031,11116,3.

基金项目

广西自然科学基金资助项目(2010GXNSFA013201). (2010GXNSFA013201)

安徽农业科学

0517-6611

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