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微乳液溶剂热法微/纳米草酸钐的合成与表征

朱文庆 袁煜昆 张文钊 许磊 王金平

纺织高校基础科学学报2012,Vol.25Issue(2):196-199,4.
纺织高校基础科学学报2012,Vol.25Issue(2):196-199,4.

微乳液溶剂热法微/纳米草酸钐的合成与表征

Synthesis and characterization of Sm2(C2O4)3 micro-/nanoparticles by microemulsion-assisted solvothermal method

朱文庆 1袁煜昆 1张文钊 1许磊 1王金平1

作者信息

  • 1. 西安工程大学环境与化学工程学院,陕西西安710048
  • 折叠

摘要

Abstract

Varies morphology and different size of Sm2(C2O4)3 were synthesized by microemulsion-assis-ted solvothermaL in which microemulsions of CTAB/l-butanol/l-octane/Sm(NO3)3 aqueous solution (K2C2O4 aqueous solution). The structures, morphologies and size of Sm2(C2O4)3 micro-/nanoparticles were characterized by X-ray diffraction (XRD), transmission electron microscope (TEM) and scanning electron microscope (SEM), respectively. The experimental results showed that the size of Sm2(C2O4)3 were increased by the the molar ratio of water to the CTAB(?) and reaction time.

关键词

微乳液溶剂热法/微/纳米草酸钐/合成与表征

Key words

mulsion-assisted Solvothermal Method/ Sm2(C2O4)3 micro-/nanoparticles/ Synthesis and characterization

分类

化学化工

引用本文复制引用

朱文庆,袁煜昆,张文钊,许磊,王金平..微乳液溶剂热法微/纳米草酸钐的合成与表征[J].纺织高校基础科学学报,2012,25(2):196-199,4.

基金项目

陕西省科技厅攻关项目(2011K07-23) (2011K07-23)

陕西省教育厅专项科研计划项目(11JK0566) (11JK0566)

西安工程大学博士基金项目(BS1010) (BS1010)

纺织高校基础科学学报

OACSTPCD

1006-8341

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