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布渣叶药材质量标准的初步研究

卢鹏 陈伟韬 陈浩桉 隆颖 杨立伟 叶文才 江仁望

广东药学院学报2012,Vol.28Issue(4):419-422,4.
广东药学院学报2012,Vol.28Issue(4):419-422,4.DOI:10.3969/j.issn.1006-8783.2012.04.016

布渣叶药材质量标准的初步研究

Study on the initial quality standard of Microcos Paniculata L.

卢鹏 1陈伟韬 1陈浩桉 2隆颖 2杨立伟 2叶文才 3江仁望3

作者信息

  • 1. 广州中医药大学中药学院,广东广州510006
  • 2. 广东省食品药品检验所,广东广州510180
  • 3. 暨南大学中药学院,广东广州510632
  • 折叠

摘要

Abstract

Objective To establish the quality standard of Microcos Paniculata L. . Methods M. Paniculata was identified with TLC, and the contents of vitexin and narcissin were determined by HPLC. Results TLC identification for M. Paniculata was established. The calibration curve was linear in the range of 0. 1 - 4 μg ( r = 0. 999 6) for vitexin and the average recovery was 96. 44% with RSD of 1. 68% ; The calibration curve was linear in the range of 0. 1 - 4 μg ( r =0. 999 6) for narcissin and the average recovery of narcissin was 97. 16% with RSD of 1. 85% . Conclustion The method of TLC and assay of the active ingredients from M. Paniculata were convenient and accurate, which may be used in its quality control.

关键词

布渣叶/TLC法/HPLC法/牡荆苷/水仙苷/质量标准

Key words

Microcos Paniculata L. / TLC/ HPLC/ vitexin/ narcissin/ quality standard

分类

医药卫生

引用本文复制引用

卢鹏,陈伟韬,陈浩桉,隆颖,杨立伟,叶文才,江仁望..布渣叶药材质量标准的初步研究[J].广东药学院学报,2012,28(4):419-422,4.

基金项目

广东省自然科学基金(835106320100O003) (835106320100O003)

广东药学院学报

OACSTPCD

1006-8783

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