河北化工2012,Vol.35Issue(9):45-46,49,3.
2-氯丙酸异丙酯的合成
Synthesis of Isopropyl 2-chloropropionate
李勇 1田青松 1张文静 1王玉东1
作者信息
- 1. 河北万全宏宇化工有限责任公司,河北张家口076271
- 折叠
摘要
Abstract
To synthesize isopropyl 2-chloropropionate with super acid resin as catalyst,and study the influences of catalyst dosage,raw material ratio,reaction time water-carrying agent varieties and dosage.The total yield was 95% and purity of the title compound was above 99% under the optimum conditions that included n(2-propanol)∶n(cyclohexane)∶n(catalyst)∶n(2-chloropropionic acid)=5∶6.5∶0.3∶1,and reaction time was 2 h.关键词
2-氯丙酸/2-氯丙酸异丙酯/合成Key words
2-chloropropionic acid/isopropyl 2-chloropropionate/synthesis分类
化学工程引用本文复制引用
李勇,田青松,张文静,王玉东..2-氯丙酸异丙酯的合成[J].河北化工,2012,35(9):45-46,49,3.