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2-氯丙酸异丙酯的合成

李勇 田青松 张文静 王玉东

河北化工2012,Vol.35Issue(9):45-46,49,3.
河北化工2012,Vol.35Issue(9):45-46,49,3.

2-氯丙酸异丙酯的合成

Synthesis of Isopropyl 2-chloropropionate

李勇 1田青松 1张文静 1王玉东1

作者信息

  • 1. 河北万全宏宇化工有限责任公司,河北张家口076271
  • 折叠

摘要

Abstract

To synthesize isopropyl 2-chloropropionate with super acid resin as catalyst,and study the influences of catalyst dosage,raw material ratio,reaction time water-carrying agent varieties and dosage.The total yield was 95% and purity of the title compound was above 99% under the optimum conditions that included n(2-propanol)∶n(cyclohexane)∶n(catalyst)∶n(2-chloropropionic acid)=5∶6.5∶0.3∶1,and reaction time was 2 h.

关键词

2-氯丙酸/2-氯丙酸异丙酯/合成

Key words

2-chloropropionic acid/isopropyl 2-chloropropionate/synthesis

分类

化学工程

引用本文复制引用

李勇,田青松,张文静,王玉东..2-氯丙酸异丙酯的合成[J].河北化工,2012,35(9):45-46,49,3.

河北化工

2095-5979

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