中医学报2012,Vol.27Issue(8):985-987,3.
熟地强筋合剂的定性鉴别和含量测定
Qualitative Identification and Content Determination of Shudi Qiangjin Mixture
摘要
Abstract
Objective;To establish the methods for qualitative identification and content determination of Shudi Qiangjin Mixture. Meth-ods : Moutan cortex and Radix glycyrrhlaze were identified by thin layer chromatography ( TLC) and the content of Loganin in corni fruc-tus was determined by high performance liquid chromatography(HPLC). Results: Moutan cortex and Radix glycyrrhlaze could be identified by TLC, which presented negativity without interference and had strong specificity. The linear range of loganin was 0.050 8-0. 304 8 μg(r =0.999 8) and had good linear relation. The average recovery rate was 98.2% ,RSD = 1.80% (n=6). Conclusion;This meth-od is simple,accurate and repeatable,which can be used in the quality control of Shudi Qiangjin Mixture.关键词
熟地强筋合剂/薄层色谱法/高效液相色谱法/含量测定/定性鉴别Key words
shudi qiangjin mixture/ thin layer chromatography (TLC) /high performance liquid chromatography ( HPLC ) / content determination / qualitative ideutificantion分类
医药卫生引用本文复制引用
刘素玲,蔡益锐..熟地强筋合剂的定性鉴别和含量测定[J].中医学报,2012,27(8):985-987,3.基金项目
广东省中医药局重点科研项目(编号:3060011) (编号:3060011)