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单面针茎中苯丙素类化学成分研究

何桂霞 梁晓岚 刘赫男 姚颖 裴刚 袁园 邹茜

湖南中医药大学学报2012,Vol.32Issue(3):38-41,4.
湖南中医药大学学报2012,Vol.32Issue(3):38-41,4.DOI:10.3969/j.issn.1674-070X.2012.03.011.038.04

单面针茎中苯丙素类化学成分研究

Study on phenylpropanoids constitunents in stem of Zanthoxylum dissitum

何桂霞 1梁晓岚 2刘赫男 1姚颖 1裴刚 1袁园 3邹茜1

作者信息

  • 1. 湖南中医药大学药学院,湖南长沙410208
  • 2. 湖南中医药大学中药现代化重点实验室,湖南长沙410208
  • 3. 如心医药(深圳)有限公司,深圳518020
  • 折叠

摘要

Abstract

Objective To study the chemical constitunents in stem of Zanthoxylum dissitum.Methods Silica gel column chromatography and recrystallization were applied for the isolation and purification of the constituents.The structures were elucidated by 1H-NMR,13C-NMR,MS and their physicochemical properties.Results From the crude ethyl alcohol fraction of the steins of Zanthoxylum dissitum,6 compounds were isolated and identified as β-sitosterol(l),vanillinβ,epis-esamin (3),(-)pluviatilol-γ,γ-dimethyallyl ether(4),fargesin(5),(-)eudesmin (6).Conclusion Compounds 2-6 were isolated and identified from the steins of Zanthoxylum dissitum for the first time.

关键词

单面针//芸香科/化学成分

Key words

Zanthoxylum dissitum/stem/Rutaceae/chemical constituents

分类

医药卫生

引用本文复制引用

何桂霞,梁晓岚,刘赫男,姚颖,裴刚,袁园,邹茜..单面针茎中苯丙素类化学成分研究[J].湖南中医药大学学报,2012,32(3):38-41,4.

基金项目

湖南省教育厅资助课题(10C1040) (10C1040)

湖南省教育厅“十二五”中药学重点学科和湖南中医药大学“十二五”药物分析学校级重点学科资助. ()

湖南中医药大学学报

OACSTPCD

1674-070X

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