生态与农村环境学报2012，Vol.28Issue(4)：451-455,5.
稻田样品中丁虫腈及其代谢产物的残留分析方法
Determination of Flufiprole and Its Metabolites in Samples From Paddy Field
摘要
Abstract
A method using solid-phase extraction and gas chromatograph-microelectron capture detector ( GC - ECD) was developed to detect flufilprole and its metabolites in plant, soil and water in paddy fields. Water samples were extracted with methylene chloride, soil samples first with acetone and then with ethyl acetate and plant samples first with acetonitrile and then with CarbonNH2 and at the end cleaned up with solid phase extraction (SPE) for analysis with GC - ECD. Results of the analysis show that the lowest content of pollutants detected was 0. 01 mg ? L-1 in the water and 0. 015 mg ? kg"' in the soil and the plant. When 0. 05 - 1. 0 mg ? L-1 (or mg ? kg-1) of the pollutants were added into the field, the recovery rate of using this method was in the range of 75. 1% - 109. 2% with variation coefficient being 1. 0% -7. 9%. This method is simple, accurate, and readily applicable in the analysis of paddy field samples.关键词
丁虫腈/测定方法/固相萃取/水稻植株/残留Key words
flufiprole/ determination method/ solid phase extraction (SPE)/ rice plant/ residue分类
资源环境引用本文复制引用
何健,孔德洋,吴文铸,宋宁慧,单正军..稻田样品中丁虫腈及其代谢产物的残留分析方法[J].生态与农村环境学报,2012,28(4):451-455,5.基金项目
国家自然科学基金(41101307) （41101307）
中央级公益性科研院所基本科研业务专项 （）
