南京工业大学学报(自然科学版)2012,Vol.34Issue(4):6-10,5.DOI:10.3969/j.issn.1671-7627.2012.04.002
块状低密度C/SiO2复合气凝胶的制备
Preparation of monolithic C/SiO2 composite aerogels with low density
摘要
Abstract
Resorcin-formaldehyde/Si02 composite ( RF/SiO2) aerogels were synthesized by the sol-gel method and CO2 supercritical fluid drying. C/SiO2 composite aerogels were formed from the RF/SiO2 aerogels after carbonization. The influence of reactant concentration on sol-gel and thermal treatment processes was investigated. The effect of heat treatment temperature on pore structure of C/SiO2 aerogels was discussed. Results showed that the heat treatment had the least impact on RF/SiO2 aerogels with the reactant concentration of 13% , and increasing the carbonization temperature to 1 200 t had an obvious improvement to the network structure of C/SiO2 aerogels.关键词
RF/SiO2气凝胶/C/SiO2气凝胶/超临界干燥/炭化/孔结构Key words
RF/SiO2 aerogels/ C/SiO2 aerogels/ supercritical drying/ carbonization/ pore structure分类
化学化工引用本文复制引用
孔勇,仲亚,沈晓冬,胡丹丹,崔升,滕凯明,张君君..块状低密度C/SiO2复合气凝胶的制备[J].南京工业大学学报(自然科学版),2012,34(4):6-10,5.基金项目
国家自然科学基金资助项目(10976013) (10976013)
江苏省自然科学基金重点资助项目(BK2010082) (BK2010082)
材料化学工程国家重点实验室开放课题基金资助项目(KL11-09) (KL11-09)
国家安全重大基础研究资助项目(613120020020202) (613120020020202)
江苏省普通高校研究生科研创新计划资助项目(CXLX11_0343) (CXLX11_0343)