印染助剂2012，Vol.29Issue(7)：8-11,4.
双活性基固色剂的合成及应用
Synthesis and application of double-reactive-group fixing agent
摘要
Abstract
Using dimethyl diallyl ammonium chloride IDMDAAC) and allyl glycidyl ether (AGE) as raw material, sodium persulfate as catalyst, environmental friendly double-reactive-group fixing agent P(DMDAAC-AGE) was synthesized. The structure and performance of P(DMDAAC-AGE) were characterized by FT-IR, TG-DTA and SEM. The main factors affecting the performance of fixing agent P(DMDAAC-AGE) were investigated. The optimum synthesis conditions were determined as follows:the mole ratio of AGE to DMDAAC 1:2, 30% of initial concentration of the monomers in water phase, 0.75% of initiator (on the mass of monomers), continuous dropwise addition of the initiator and AGE, reacted at 80 ℃ for 6 h. The reactive dyed cotton fabric fixed by P(DMDAAC-AGE) had fairly good color fastness with 4-level to wet rubbing, 4~5-level to dry rubbing and 4-level to soaping.关键词
二甲基二烯丙基氯化铵/烯丙基缩水甘油醚/固色剂/活性染料/合成/应用Key words
dimethyl diallyl ammonium chloride/ allyl glycidyl ether/ fixing agent/ reactive dyes/ synthesis/ application分类
化学化工引用本文复制引用
史亚鹏,周向东,张海玲,王丽,朱敏..双活性基固色剂的合成及应用[J].印染助剂,2012,29(7):8-11,4.基金项目
江苏高校优势学科建设工程资助项目(PAPD) （PAPD）
