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二氧化硅负载磷钨酸催化合成月桂酸乙酯

王芬华 黄江胜 李芳 刘超

安徽工程大学学报2012,Vol.27Issue(3):4-5,9,3.
安徽工程大学学报2012,Vol.27Issue(3):4-5,9,3.

二氧化硅负载磷钨酸催化合成月桂酸乙酯

Catalytic synthesis of ethyl laurate with silion dioxide supported on phosphotungstic acid

王芬华 1黄江胜 2李芳 1刘超1

作者信息

  • 1. 安徽工程大学生物与化学工程学院,安徽芜湖241000
  • 2. 安徽工程大学机电学院,安徽芜湖241000
  • 折叠

摘要

Abstract

Ethyl Laurate was synthesized by using silicon dioxide as catalyst supported on phosphotung- stic acid. The effects of the molar ration of lauric acid to alcohol,mass of catalyst,reaction time and tem- perature on the yield were investigated. Experimental results show that silicon dioxide supported on phosphotungstic acid was an excellent catalyst. The yield was over 80% under optimum condition. The suitable conditions were that molar ratio of laurie acid to alcohol is 1 : 5, amount of catalys is 6.0% of the lauric acid,reaction temperature is 90 ℃ and reaction time is 4.0 h.

关键词

月桂酸乙酯/磷钨酸/负载/催化

Key words

ethyl laurate/phosphotungstic acid/supported on/catalytic synthesis

分类

化学化工

引用本文复制引用

王芬华,黄江胜,李芳,刘超..二氧化硅负载磷钨酸催化合成月桂酸乙酯[J].安徽工程大学学报,2012,27(3):4-5,9,3.

基金项目

安徽省教育厅基金资助项目 ()

安徽工程大学学报

2095-0977

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