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飞行时间质谱仪传输区射频电源的研制

谢春光 郭长娟 王姜 江宗耀 高伟 黄正旭 傅忠 周振

分析测试学报2012,Vol.31Issue(8):922-927,6.
分析测试学报2012,Vol.31Issue(8):922-927,6.DOI:10.3969/j.issn.1004-4957.2012.08.006

飞行时间质谱仪传输区射频电源的研制

Development of a Radio Frequency Power Supply for Radio Frequency Quadrupole in Time-of-flight Mass Spectrometer

谢春光 1郭长娟 2王姜 3江宗耀 4高伟 1黄正旭 1傅忠 3周振1

作者信息

  • 1. 上海大学环境与化学工程学院环境污染与健康研究所,上海200072
  • 2. 华南师范大学化学与环境学院,广东广州510006
  • 3. 广州禾信分析仪器有限公司,广东广州510663
  • 4. 东华理工大学江西省质谱科学与仪器重点实验室,江西南昌330013
  • 折叠

摘要

Abstract

A new radio frequency(RF) power supply was developed, which composed of the module of signal generating and amplifying, the module of amplitude adjusting and the module of power driving. The power supply is compact, small size, stable and low cost, and is divided into low-frequency part and high-frequency part to drive two radio frequency quadrupoles in home-made time-of-flight mass spectrometer. The tunable frequency range of RF power supply are 150 - 900 kHz in low-frequency and 1-2 MHz in high frequency, the adjustable range of peak to peak voltage Vp_p are 0 -100 V in low-frequency and 0-1 400 V in high frequency. With the RF power supply described in this paper, the home-made time-of-flight mass spectrometer was used to test the samples. As a result , the ions with m/z of 50 -1 200 could be stably measured, and a good linearity was obtained in the concentration range of 5. 0 × 10 -9 - 5. 0 ×10-5 mol/L for samples.

关键词

射频电源/射频四极杆/飞行时间质谱仪

Key words

radio frequency power supply/ radio frequency quadrupole (RFQ)/ time-of-flight mass spectrometer(TOF MS)

分类

机械制造

引用本文复制引用

谢春光,郭长娟,王姜,江宗耀,高伟,黄正旭,傅忠,周振..飞行时间质谱仪传输区射频电源的研制[J].分析测试学报,2012,31(8):922-927,6.

基金项目

国家自然科学基金项目(21105031) (21105031)

国家重大科学仪器设备开发专项(2011YQ17006703) (2011YQ17006703)

分析测试学报

OA北大核心CSCDCSTPCD

1004-4957

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