火炸药学报Issue(4)：26-29,4.
苯并三氧化呋咱的晶体结构
Crystal Structure of Benzotrifuroxan
周彦水 1王锡杰 1周诚 1霍欢 1张毅 2王伯周 1张叶高 1苏鹏飞1
作者信息
- 1. 西安近代化学研究所,陕西西安710065
- 2. 边防学院,陕西西安710108
- 折叠
摘要
Abstract
The single crystal of benzotrifuroxan (BTF) was cultured using the mixed solvent of water and methanol. BTF was characterized by using the X-ray single-crystal diffraction analysis, mass spectrometry, nuclear magnetic resonance spectrometry, element analysis and FT-IR technique. The results show that the crystal is orthorhombic system, space group P2 (1) , with crystal parameters of a = 0. 6935(12)nm,b= 1. 9557(3)nm,c = 0. 6518(ll)nm,V= 0. 884(3)nm3,Z=4,Dc = l. 894 g/cm3 μ=0. 173 mm-1 ,F(000) = 504 ,R1 =0. 0313, wR2 =0. 0723. The BTF molecule is planar.关键词
物理化学/含能化合物/苯并三氧化呋咱/晶体结构Key words
physical chemistry/ energetic compound/ benzotrifuroxan/ crystal structure分类
军事科技引用本文复制引用
周彦水,王锡杰,周诚,霍欢,张毅,王伯周,张叶高,苏鹏飞..苯并三氧化呋咱的晶体结构[J].火炸药学报,2012,(4):26-29,4.
