林产化学与工业2012，Vol.32Issue(4)：97-101,5.
马来海松酸锌的合成及表征
Synthesis and Characterization of Zincum Maleopimarate
摘要
Abstract
Zincum maleopimarate (MPAZn) has been synthesized from maleopimaric acid and zinc acetate with solvent method. The influence of reaction conditions such as amount of raw material, reaction time, reaction temperature on product were discussed respectively. Zinc content in the products was determined by complexometric titration. The target product was analyzed and characterized by Fourier transform infrared spectrometer (FT-IR) , Scanning electron microscope (SEM) , Energy dispersive X-ray microanalysis (EDAX) analysis and X-ray diffraction (XRD). The optimum reaction conditions were ascertained as follows : n ( zinc acetate ) : n ( maleopimaric acid) = 3 : 1 , at 328 K for 5 h, the yield of MPAZn could reach 94 % . It was found that MPAZn was three-dimensional reticulation compound and chemical bonding occurs between the -COO- and Zn2+.关键词
马来海松酸酐/松香/马来海松酸锌Key words
maleopimaric anhydride/rosin/Zincum maleopimarate分类
化学化工引用本文复制引用
杨忠芝,黄奇良,雷福厚..马来海松酸锌的合成及表征[J].林产化学与工业,2012,32(4):97-101,5.基金项目
广西自然科学基金资助项目(桂科自0542019) （桂科自0542019）
广西高校人才小高地科研基金资助项目(无编号) （无编号）
