生命科学仪器2012，Vol.10Issue(5)：19-21,3.
毛细管气相色谱法测定海参口服液中甲基汞的含量
Determination of Methylmercury in Sea Cucumber Oral Liquid by Capillary GC
鲁刚 1宗万里1
作者信息
- 1. 威海市产品质量监督检验所,山东威海264209
- 折叠
摘要
Abstract
The method is established for the determination of Methylmercury in Sea Cucumber Oral Liquid by Capillary GC. The separation was achieved by using WBI injection port, Capillary GC column DB-5(weak polarity,30m ×0.53 mm × 0.5 μm), ECD detector. Injecton port temperature: 200℃, flow of carrier gas:10 mL/min, column oven temperature: 100℃ keep 2 min, then 5℃/min up to 230℃, detector temperature: 300℃. The method is accurate, rapid and convenient. The results indicate that the recovery is more than 85%, RSD is less than 3.0% and the working curve of Methylmercury is in the linear range 0.1 μ g/mL- 1.0 μ g/mL.关键词
毛细管气相色谱法/海参口服液/甲基汞Key words
Capillary GC/Sea Cucumber Oral Liquid/Methylmercury.分类
化学化工引用本文复制引用
鲁刚,宗万里..毛细管气相色谱法测定海参口服液中甲基汞的含量[J].生命科学仪器,2012,10(5):19-21,3.
