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多孔纳米钡铁氧体制备及其吸附铀的性能研究

熊国宣 黄海清 张志宾

原子能科学技术2012,Vol.46Issue(9):1041-1044,4.
原子能科学技术2012,Vol.46Issue(9):1041-1044,4.

多孔纳米钡铁氧体制备及其吸附铀的性能研究

Preparation of Porous Nano Barium Ferrite and Its Adsorption Properties on Uranium

熊国宣 1黄海清 2张志宾1

作者信息

  • 1. 东华理工大学放射性地质与勘探技术国防重点学科实验室,江西抚州344000
  • 2. 核资源与环境教育部重点实验室(东华理工大学),江西南昌 330013
  • 折叠

摘要

Abstract

The porous nano barium ferrite was made of Fe(NO3)3 and Ba(NO3)2 as raw materials, CTAB as surfactant by method of sol-gel and self-propagating combustion. The composition, morphology and magnetic properties of nano-rod barium ferrite were characterized by XRD, SEM and vibrating sample magnetometer. The adsorption properties of porous nano barium ferrite on uranium were studied with static adsorption and the effects of pH, adsorption temperature and oscillation time on adsorption properties were discussed. The results indicate that the average particle size of porous nano barium ferrite is 45-65 nm, the saturation magnetization and coercivity are 62. 83 emu/g and 5 481. 0 Oe, respectively. Under the condition of the porous nano barium ferrite amount of 0. 02 g, pH of 6, adsorption temperature of 25 ℃ and oscillation time of 30 min, the adsorption capacity of uranium on the porous nano barium ferrite reaches 921 μ/g.

关键词

多孔纳米钡铁氧体/制备/吸附性能/

Key words

porous nano barium ferrite/ preparation/ adsorption property/ uranium

分类

信息技术与安全科学

引用本文复制引用

熊国宣,黄海清,张志宾..多孔纳米钡铁氧体制备及其吸附铀的性能研究[J].原子能科学技术,2012,46(9):1041-1044,4.

基金项目

放射性地质与勘探技术国防重点学科实验室开放基金资助项目(2010RGET04) (2010RGET04)

江西省自然科学基金资助项目(2009GZC0001) (2009GZC0001)

原子能科学技术

OA北大核心CSCDCSTPCD

1000-6931

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