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能量色散X射线荧光光谱法同时测定涂料中的铅、铬、镉、汞

周衡刚 邓思娟

合成材料老化与应用2012,Vol.41Issue(5):29-31,3.
合成材料老化与应用2012,Vol.41Issue(5):29-31,3.

能量色散X射线荧光光谱法同时测定涂料中的铅、铬、镉、汞

Simultaneous Determination of Pb, Cr, Cd and Hg in Paints by Energy-Dispersive X-Ray Fluorescence Spectroscopy

周衡刚 1邓思娟1

作者信息

  • 1. 广州合成材料研究院有限公司,广东广州510665
  • 折叠

摘要

Abstract

In this paper,ED-XRF (Energy-dispersive X-ray fluorescence spectrometry) spectrometric method for the determination of Pb,Cr,Cd,Hg in paints has been established . The experimental results showed a good linear relationship in the concentration range from25 mg/kg to 200 mg/kg . The detection limits were 13,7,4 mg/kg and 9 mg/kg for Pb,Cr,Cd and Hg,respectively. The recovery rates and the relative standard deviation of the method were in the range of 91. 8% - 101. 6% and 1. 2% -4. 3% .respectively. As compared with national standard methods for the determination of Pb,Cr,Cd,Hg in paints,this method is simpler,faster and satisfied the semi-quantitative determination of Pb,Cr,Cd,Hg in paints with good accuracy and detection limits,can be applied to the heavy metals inspection in paints.

关键词

能量色散X射线荧光光谱法/涂料/重金属/检测

Key words

Energy-dispersive X-ray Fluorescence Spectroscopy/Paint/Heavy Metal/Determination

分类

化学化工

引用本文复制引用

周衡刚,邓思娟..能量色散X射线荧光光谱法同时测定涂料中的铅、铬、镉、汞[J].合成材料老化与应用,2012,41(5):29-31,3.

合成材料老化与应用

OACSTPCD

1671-5381

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