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微波辐照废木屑活性炭制备工艺优化及其应用

蒋莉 马飞 叶招莲 张国华 周蕾

环境工程学报2012,Vol.6Issue(12):4661-4665,5.
环境工程学报2012,Vol.6Issue(12):4661-4665,5.

微波辐照废木屑活性炭制备工艺优化及其应用

Optimization of activated carbons production from waste sawdust via microwave heating and its application

蒋莉 1马飞 2叶招莲 1张国华 1周蕾1

作者信息

  • 1. 江苏技术师范学院化学与环境工程学院,常州213001
  • 2. 江苏技术师范学院化学与环境工程学院,常州213001 河海大学水利水电工程学院,南京210098
  • 折叠

摘要

Abstract

Microwave was used as a heat source in preparing activated carbon (AC) from waste sawdust by Na2CO3 chemical activation in this study. Taguchi method was used to investigate effects of microwave power, microwave radiation time, Na2CO3 solution concentration and solid-to-liquid ratios on iodine value. Results re- vealed that microwave power was the most important factor, followed by radiation time. However, solid-to-liquid ratios had no significant effect. The optimized technological parameters were as follows: microwave power of 440 W, microwave radiation time of 9 rain, Na2 CO3 solution concentration of 15 % and solid-to-liquid ratios of 1:2.5, iodine value was up to 1 230.40 mg/g. Adequacy of model equation for predicting optimal response values was verified effectively by validation. Furthermore, the prepared AC was applied to wastewater treatment, and results showed that, with 3 g/L mass fraction addition of AC, the COD removal rate of wastewater was 77.9% after 70 min adsorption at pH 11.

关键词

废木屑/活性炭/微波法/Na2CO3Taguchi法

Key words

waste sawdust/activated carbon/microwave/Na2CO3/Taguchi method

分类

资源环境

引用本文复制引用

蒋莉,马飞,叶招莲,张国华,周蕾..微波辐照废木屑活性炭制备工艺优化及其应用[J].环境工程学报,2012,6(12):4661-4665,5.

基金项目

国家自然科学基金资助项目 ()

江苏省高校自然科学基金 ()

江苏技术师范学院基础及应用基础项目 ()

环境工程学报

OA北大核心CSCDCSTPCD

1673-9108

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