中医药导报2012，Vol.18Issue(9)：85-87,3.
病毒清口服液的质量标准研究
Study on Quality Standards of Bingduqing Oral Liquid
湛延风 1付红伟 2何亚辉3
作者信息
- 1. 岳阳市第二人民医院,湖南岳阳414000
- 2. 岳阳市中医院,湖南岳阳414000
- 3. 湖南省中医药研究院,湖南长沙410006
- 折叠
摘要
Abstract
Objective: To establish a quality standard for Bingduqing Oral Liquid. Methods: TLC was used to identify Fructus Citri Sarcodactylis, licorice and honeysuckle in Bingduqing Oral Liquid. HPLC was applied to determine the Phillyrin in Pursue; The separation was performed on a C18ODS-Clg column (200 mm×4.6 mm, 5 μm); The mobile phase was consisted of acetonitrile and water(25:75); The detection wavelength was 277 nm; Flow rate was 1 mL per minute; Column temperature was 25 ℃. Results: The Fructus Citri Sarcodactylis, licorice and honeysuckle in Bingduqing Oral Liquid showed the same color brindle in TLC as that of the Control medicines. The linear relations for Phillyrin in control medicines was good, SD in 0.0082-0.082 μg, r=0.9997; The average recovery of the added index was 99.63%; the RSD% was 0.96%. Conclusion: The method is reproducible and accurate to the quality control for this medicine.关键词
病毒清口服液/绿原酸/HPLC/TLC/质量标准Key words
Bingduqing Oral Liquid/ Chlorogenic Acid/ HPLC/ TLC/ Standard for Quality分类
医药卫生引用本文复制引用
湛延风,付红伟,何亚辉..病毒清口服液的质量标准研究[J].中医药导报,2012,18(9):85-87,3.
