华中师范大学学报（自然科学版）2012，Vol.46Issue(5)：560-564,5.
无溶剂法合成新型含硅离子液体
Solvent-free synthesis of novel silicon containing inonic liquids
摘要
Abstract
A series of novel l-trimethylsilylmethyl-3-alkylimidazolium inonic liquids were synthesized in 86%~97% yields from imidazole or N-methylimidazole using solvent-free method. It was investigated the effect of the reaction time, temperature and the mole ratio of the reactants on the yields, and obtained an optimized reaction condition. The results showed solvent-free method had more simple procedure and convenient work-up, and met the requirement of green chemistry. The structures of the compounds were confirmed by 'H NMR, R and IR.关键词
离子液体/合成/无溶剂法Key words
inonic liquids/ synthesis/ solvent-free分类
化学化工引用本文复制引用
唐子龙,易芳文,唐瑞仁,夏赞稳,刘汉文..无溶剂法合成新型含硅离子液体[J].华中师范大学学报（自然科学版）,2012,46(5):560-564,5.基金项目
湖南省自然科学基金(11JJ3016) （11JJ3016）
湖南省教育厅重点项目(10A034) （10A034）
理论化学教育部重点实验室开放基金(LKF0906) （LKF0906）
中南大学博士后科学基金. （）
