人工晶体学报2012,Vol.41Issue(4):900-904,915,6.
催化剂焙烧温度对热解火焰法合成碳纳米管的影响
Influence of Catalyst Calcination Temperature on Flame Pyrolysis Synthesis of Carbon Nanotubes
摘要
Abstract
In flame pyrolysis synthesis, carbon nanotubes were obtained using substrate-supported catalyst Fe/Mo/Al2O3 and CO as carbon feedstock. To study the influence of calcination temperatures in the procedure of catalyst, six experimental conditions were designed. The morphology and microscopic structure of samples were characterized by scanning electron microscopy and Raman spectrometer. Analysis shows, under this experimental conditions, with the calcination temperature being about 800-1000℃ , carbon nanotubes samples have a better quality and yield. When the catalysts were baked at about 900℃, single-wall carbon nanotubes of high quality were synthesized.关键词
碳纳米管/热解火焰/催化剂/焙烧温度Key words
carbon nanotubes/ flame pyrolysis/ catalyst/ calcination temperature分类
通用工业技术引用本文复制引用
孙保民,袁媛,郭永红,贾斌,王阳..催化剂焙烧温度对热解火焰法合成碳纳米管的影响[J].人工晶体学报,2012,41(4):900-904,915,6.基金项目
中央高校基本科研业务费专项资金资助 ()