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催化剂焙烧温度对热解火焰法合成碳纳米管的影响

孙保民 袁媛 郭永红 贾斌 王阳

人工晶体学报2012,Vol.41Issue(4):900-904,915,6.
人工晶体学报2012,Vol.41Issue(4):900-904,915,6.

催化剂焙烧温度对热解火焰法合成碳纳米管的影响

Influence of Catalyst Calcination Temperature on Flame Pyrolysis Synthesis of Carbon Nanotubes

孙保民 1袁媛 1郭永红 1贾斌 1王阳1

作者信息

  • 1. 华北电力大学电站设备状态监测与控制教育部重点实验室,北京102206
  • 折叠

摘要

Abstract

In flame pyrolysis synthesis, carbon nanotubes were obtained using substrate-supported catalyst Fe/Mo/Al2O3 and CO as carbon feedstock. To study the influence of calcination temperatures in the procedure of catalyst, six experimental conditions were designed. The morphology and microscopic structure of samples were characterized by scanning electron microscopy and Raman spectrometer. Analysis shows, under this experimental conditions, with the calcination temperature being about 800-1000℃ , carbon nanotubes samples have a better quality and yield. When the catalysts were baked at about 900℃, single-wall carbon nanotubes of high quality were synthesized.

关键词

碳纳米管/热解火焰/催化剂/焙烧温度

Key words

carbon nanotubes/ flame pyrolysis/ catalyst/ calcination temperature

分类

通用工业技术

引用本文复制引用

孙保民,袁媛,郭永红,贾斌,王阳..催化剂焙烧温度对热解火焰法合成碳纳米管的影响[J].人工晶体学报,2012,41(4):900-904,915,6.

基金项目

中央高校基本科研业务费专项资金资助 ()

人工晶体学报

OA北大核心CSCDCSTPCD

1000-985X

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