人工晶体学报2012，Vol.41Issue(5)：1227-1231,5.
声化学法制备FeVO4微晶及其光学性能
Optical Property of FeVO4 Crystallites Synthesized by Sonochemical Method
摘要
Abstract
FeVO4 crystallites were prepared by sonochemical method using NH4VO3 and Fe( NO3)3 ·9H2O as source precursors. The phase, morphology and optical properties of as-prepared samples were characterized by XRD, SEM, UV-vis absorption spectra and DSC. The results show that the synthesized FeVO4 crystallites have triclinic structure. The particle size of the crystallites decrease gradually and change more uniformity with the increase of ultrasonic irradiation power from 300 W to 500 W. UV-vis absorption spectra show that FeV04 crystallites exhibit strong absorption in visible band, the grain size decreases and the corresponding bandgaps decrease about from 2. 17 eV to 2. 08 eV with the increase of ultrasonic irradiation power.关键词
FeVO4微晶/声化学法/光学性能Key words
FeVO4 crystallites/ sonochemical method/ optical property分类
数理科学引用本文复制引用
李阿婷,曹丽云,黄剑锋,黄毅成,吴建鹏..声化学法制备FeVO4微晶及其光学性能[J].人工晶体学报,2012,41(5):1227-1231,5.基金项目
国家自然科学基金(51102196) （51102196）
陕西省国际科技合作重点项目(2011KW-11) （2011KW-11）
陕西省自然科学基金(2010JM6001) （2010JM6001）
陕西省教育厅专项项目(2010JK444) （2010JK444）
陕西省教育厅自然科学专项基金(09JK361) （09JK361）
