人工晶体学报2012，Vol.41Issue(5)：1250-1253,4.
氧化锌微米棱棒的水热法制备和稀土掺杂
Hydrothermal Synthesis of ZnO and Rare-earth Doped ZnO Micro-prisms
摘要
Abstract
The ZnO micro-prisms with different morphology and Er3+ doped ZnO samples have been synthesized via a hydrothermal method by tuning the solvent. The prepared ZnO samples were characterized by powder X-ray diffraction ( XRD ) , scanning electron microscopy ( SEM ) , photoluminescence (PL) spectrometer and spectrophotometry. The results indicated that uniform micro-prisms can be easily obtained by tuning the volume ratio of alcohol to water. When the volume ratio of alcohol to water is 1 : 2. 5 , the ZnO samples have the weakest defects emission, the lowest defects concentration and the best crystalline quality. The absorptivity increases with the increase of Er concentration until the concentration of Er + reaches to 4mol% .关键词
水热法/氧化锌/光学性能Key words
hydrothermal method/ ZnO/ optical property分类
机械制造引用本文复制引用
王洪洪,陈永生,周建朋,何伟,卢景霄..氧化锌微米棱棒的水热法制备和稀土掺杂[J].人工晶体学报,2012,41(5):1250-1253,4.基金项目
国家重点基础研究发展计划(973计划)(2011CBA00706) （973计划）
国家自然科学基金(51007082) （51007082）
河南省基础与前沿技术研究计划项目(102300410075) （102300410075）
