现代科学仪器Issue(5)：126-128,3.
湿法消化ICP-MS法与微波消解ICP-MS法测定圆白菜标准物质中铅、镉、砷的比较
Determination Comparison of Pb,Cd,and As in Standard Materials of Cabbage by ICPMS with Wet Digestion and Microwave Digestion
马小宁 1熊伟1
作者信息
- 1. 农业部食品质量监督检验测试中心石河子,新疆石河子832000
- 折叠
摘要
Abstract
A method was developed for the determination of Pb,Cd,and As in standard materials of Cabbage by inductively coupled plasma mass spectrometry(ICP-MS).After the two pretreatment methods of wet digestion and microwave digestion,the samples were directly determined by ICP-MS with on-line interna1 standard to correct the the instrument signal drift.Comparig determination results on elements of Pb,Cd,As determinated by two pretreatment methods,their detemination value has no significant difference with the reference value range.The relative standard deviation is between 0.41-4.0%,the result is accurate and reliable.Two pretreatment methods all can be used as ICP-MS pretreatment methods.关键词
湿法消化/微波消解/电感耦合等离子体质谱法（ICP-MS）Key words
Wet digestion/Microwave digestion/Inductively coupled plasma mass spectrometry(ICP-MS)分类
化学化工引用本文复制引用
马小宁,熊伟..湿法消化ICP-MS法与微波消解ICP-MS法测定圆白菜标准物质中铅、镉、砷的比较[J].现代科学仪器,2012,(5):126-128,3.
