河北科技大学学报2012，Vol.33Issue(5)：397-399,405,4.
4-(4-甲基苯氧基)苄胺的合成研究
Synthesis of 4-(4-methylphenoxy) benzylamine
摘要
Abstract
4-(4-methylphenoxy)benzylamine was synthesized by the reaction of etherification and reduction with the starting materials of p- chlorobenzonitrile and p-cresol. The target compound was identified by IR and NMR The total yield of the title compound is 69. 3%, which is obtained under optimized conditions: n(NaBH1): n(BF3-Et2O) : n(4-(4-methylphenoxy) ben-zonitrile) = l. 2 : 1. 0 : 1. 0, reaction temperature of reflux condition and reaction time of 18 h. The present method has the advantages of availability of starting materials, mild reaction condition, convenient manipulation, non-special equipment and good yield.关键词
对氯苯甲腈/4-(4-甲基苯氧基)苄胺/还原Key words
p-chlorobenzonitrile/ 4-(4-methylphenoxy)benzylamine/ reduction分类
化学化工引用本文复制引用
陈韶蕊,李爱军,陈明明..4-(4-甲基苯氧基)苄胺的合成研究[J].河北科技大学学报,2012,33(5):397-399,405,4.基金项目
河北省科技支撑计划项目(10212160) （10212160）
河北省自然科学基金资助项目(B2012208036) （B2012208036）
