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Ni-Fe-P合金催化制备螺旋碳纤维

史海林 寇开昌 高攀 卓龙海

宇航材料工艺2012,Vol.42Issue(6):56-59,64,5.
宇航材料工艺2012,Vol.42Issue(6):56-59,64,5.

Ni-Fe-P合金催化制备螺旋碳纤维

Preparation of Carbon Micro-Coils Using Ni-Fe-P Alloy as Catalyst

史海林 1寇开昌 1高攀 1卓龙海1

作者信息

  • 1. 西北工业大学理学院应用化学系,西安710129
  • 折叠

摘要

Abstract

The Ni-Fe-P alloy catalysts were deposited on the graphite matrix using electroless plating method, the catalysts were also characterized and analyzed by scanning electron microscopy, X-ray diffraction, energy dispersive X-ray. Using the heat treated Ni-Fe-P alloy as catalyst, thiophene as impurity, acetylene as the carbon source, the carbon micro-coils were successfully prepared by chemical vapor deposition method under the reaction temperature at 650℃. The study found that the resulting products are almost a regular dimension, morphology of the double helix carbon fibers, the length of the fiber is millimeter, the helix diameter and the single fiber diameter are 2 to 3 μm,0. 5 to 0. 8 μm.

关键词

合金催化剂/化学气相沉积/螺旋碳纤维

Key words

Alloy catalyst/ Chemical vapor deposition/ Carbon micro-coils

引用本文复制引用

史海林,寇开昌,高攀,卓龙海..Ni-Fe-P合金催化制备螺旋碳纤维[J].宇航材料工艺,2012,42(6):56-59,64,5.

基金项目

西北工业大学研究生创业种子基金(Z2012153) (Z2012153)

宇航材料工艺

OA北大核心CSCDCSTPCD

1007-2330

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