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阿扑西林结构确证的谱学研究

孙学伟 李志刚 倪广才 徐春霞 丁锐 余立

波谱学杂志2012,Vol.29Issue(4):582-589,8.
波谱学杂志2012,Vol.29Issue(4):582-589,8.

阿扑西林结构确证的谱学研究

Spectral Studies and Structural Elucidation of Aspoxicillin

孙学伟 1李志刚 1倪广才 1徐春霞 1丁锐 2余立2

作者信息

  • 1. 北京福瑞康正医药技术研究所,北京 100039
  • 2. 北京市药品检验所,北京 100035
  • 折叠

摘要

Abstract

The infrared spectrum, ultraviolet spectrum, nuclear magnetic resonance spectra and mass spectra of aspoxicillin, a semi-synthetic penicillin, were collected and interpreted. All the NMR signals were assigned. Based on the mass spectral data, the possible fragmentation pathways were discussed. The infrared spectrum was used to analyze the types of vibration of the functional groups in this compound. The structure of the compound was determined.

关键词

核磁共振(NMR)/结构确证/阿扑西林/红外光谱/紫外光谱/质谱

Key words

NMR/ structure elucidation/ aspoxicillin/ infrared spectroscopy/ ultraviolet spectroscopy/ mass spectroscopy

分类

数理科学

引用本文复制引用

孙学伟,李志刚,倪广才,徐春霞,丁锐,余立..阿扑西林结构确证的谱学研究[J].波谱学杂志,2012,29(4):582-589,8.

基金项目

科技型中小企业技术创新基金资助项目(09C26211102765). (09C26211102765)

波谱学杂志

OA北大核心CSCDCSTPCD

1000-4556

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