河北工业科技2013,Vol.30Issue(1):1-5,5.DOI:10.7535/hbgykj.2013yx0101
Zr-Al合金化学镀Ni-P镀层工艺研究
Study of electroless Ni-P plating on Zr-Al alloy
摘要
Abstract
The purpose of this paper is to get the electroless Ni-P plating on the surface of Zr-8 Al alloy. The Ni-P plating was even, cystiform and amorphous. The ingredient of phosphating solution was obtained as follows: 15 g/L H3PO4, 3 g/L ZnSO4, 1. 5 g/L NaF, 0.15 g/L organic amine. Phosphating was carried at 45℃ for 2 minutes with pH value of 2. 5~3. 0. The ingredient of electroless bath was: 20 g/LNiSO4,40 g/LNaH2PO2, 40 g/L(NH4)2SO4,40 g/L CH3COONa, 1 mg/L (CH3COO)2Pb. Electroless plating was carried at 80℃ for 1 hour with pH value of 5. 5~6. 0. From microhardness, electrochemical polarization, XRD and SEM results, it is shown that the corrosion resistance and microhardness of Zr-Al alloy with Ni-P plating were remarkably improved.关键词
Zr-Al合金/化学镀Ni-P/磷化处理/显微硬度/耐蚀性Key words
Zr-Al alloy/ electroless Ni-P plating/ phosphating pretreating/ microhardness/ corrosion resistance分类
矿业与冶金引用本文复制引用
秦文波,马静,李强,张双杰,李永刚,李扬..Zr-Al合金化学镀Ni-P镀层工艺研究[J].河北工业科技,2013,30(1):1-5,5.基金项目
国家973项目(2010CB731604) (2010CB731604)
河北科技大学杰出青年基金项目 ()
河北科技大学大学生科技创新基金项目 ()