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一种快速分析土壤样品中90Sr的方法

舒复君 杨金玲 杨志红 丁有钱 梁小虎 张生栋

核化学与放射化学2013,Vol.35Issue(1):14-18,5.
核化学与放射化学2013,Vol.35Issue(1):14-18,5.DOI:10.7538/hhx.2013.35.01.0014

一种快速分析土壤样品中90Sr的方法

A Rapid Method for Radiochemical Analysis of 90Sr in Soils

舒复君 1杨金玲 1杨志红 1丁有钱 1梁小虎 1张生栋1

作者信息

  • 1. 中国原子能科学研究院放射化学研究所,北京102413
  • 折叠

摘要

Abstract

90Sr in many soil samples should be analyzed, so that radioactive pollution level in nuclear facilities and its surrounding environment can be surveyed efficiently. In this paper, a rapid radioanalytical method of 90Sr in soils was developed. The main procedures consist of pretreatment, oxalate precipitation, Sr·Spec resin chromatographic separation, and radioactivity determination by time correction or dual labeling method using liquid scintillation spectrometry. Typically, a sample can be analyzed in 6 h. The chemical yield is about 60% , and the minimum detectable activity by this technique is about 8 Bq/kg.

关键词

土壤/90Sr/Sr·Spec树脂/液闪测量

Key words

soils/ 90Sr/ Sr·Spec resin/ liquid scintillation spectrometry

分类

化学化工

引用本文复制引用

舒复君,杨金玲,杨志红,丁有钱,梁小虎,张生栋..一种快速分析土壤样品中90Sr的方法[J].核化学与放射化学,2013,35(1):14-18,5.

核化学与放射化学

OA北大核心CSCD

0253-9950

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