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微波消解-GFAAS法测定土壤中的总铅

马小宁 姬勇

环境保护科学2013,Vol.39Issue(1):58-60,3.
环境保护科学2013,Vol.39Issue(1):58-60,3.

微波消解-GFAAS法测定土壤中的总铅

Determination of Total Lead Contents in Soil by Microwave Digestion-GFAAS

马小宁 1姬勇1

作者信息

  • 1. 农业部食品质量监督检验测试中心,新疆石河子832000
  • 折叠

摘要

Abstract

It studied a method of microwave digestion-GFAAS for the determination of total lead in soil. HNO3 and HF were added into the soil samples,the microwave digestion under the certain condition was conducted and in a constant temperature heater to drive acid and remove silicon, then total lead content in soil was determined by Graphite Furnace Atomic Absorption Spectrometric(GFAAS) method. Compared with the national standard (GB/T 17141-1997) digestion method ,and determined the different soil and soil standard substances, the results show that: the two methods have no significant difference. This method is well repeatable, with less reagent dosage, safe and easy to control and it is reliable.

关键词

微波消解/石墨炉原子吸收法(GFAAS)/土壤/

Key words

Microwave Digestion/ Graphite Furnace Atomic Absorption Spectrometry ( GFAAS ) / Soil/ Lead

分类

资源环境

引用本文复制引用

马小宁,姬勇..微波消解-GFAAS法测定土壤中的总铅[J].环境保护科学,2013,39(1):58-60,3.

环境保护科学

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