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间歇萃取精馏分离叔丁醇与水共沸物的研究

缪英 张春林 叶青

常州大学学报(自然科学版)2012,Vol.24Issue(4):33-36,4.
常州大学学报(自然科学版)2012,Vol.24Issue(4):33-36,4.

间歇萃取精馏分离叔丁醇与水共沸物的研究

Study of Separating Tert-Butyl Alcohol-Water by Batch Extractive Distillation

缪英 1张春林 2叶青2

作者信息

  • 1. 常州大学基建处,江苏常州213164
  • 2. 上海制皂(集团)如皋有限公司,江苏如皋226521
  • 折叠

摘要

Abstract

Batch extractive distillation process was chosen to separate tert—butyl alcohol —water mixture and the ethylene glycol as solvent. The effect of reflux ratio, solvent feeding speed and solvent feeding temperature was analyzed. The best operating conditions were that the reflux ratio was 2, solvent feeding speed was 5. Lg/min, the solvent feeding temperature was 90℃. Under those conditions, the mass fraction of tert —butyl alcohol could reach 98. 41%. The batch extractive distillation column was simulated by Aspen plus software, and an agreement was found between the predicted and the experimental data.

关键词

叔丁醇/间歇萃取精馏/模拟

Key words

tert—butyl alcohol/ batch extractive distillation/ simulation

分类

化学化工

引用本文复制引用

缪英,张春林,叶青..间歇萃取精馏分离叔丁醇与水共沸物的研究[J].常州大学学报(自然科学版),2012,24(4):33-36,4.

常州大学学报(自然科学版)

2095-0411

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