矿产综合利用Issue(1):54-57,4.DOI:10.3969/j.issn.1000-6532.2013.01.014
低能耗型可膨胀石墨的制备研究
Study on Preparation of Low Energy Consumption Type Expandable Graphite
周丹凤 1田金星1
作者信息
- 1. 武汉理工大学资源与环境工程学院,湖北武汉430070
- 折叠
摘要
Abstract
The HClO4/CH3C00H/KMnO4 oxidation intercalation system for preparing low temperature expandable graphite was developed in this paper. To obtain the optimum conditions and the material proportion, the influence of the dosage of perchloric acid, acetic acid and potassium permanganate, reaction temperature and reaction time was studied. When the reaction was carried out at 35℃ for 60min, and the optimal mass ratio of graphite(g) , perchloric acid(mL) , acetic acid(mL)and potassium permangantate(g) was 1 : 4 : 1. 5 : 0. 15 ,the inflation volume of grapite could attain 423mL/g at 400℃. There were not any sulfur-containing reagents,so the expansible graphite did not contain sulfur.关键词
低能耗/可膨胀石墨/制备/膨胀容积Key words
Low energy consumption/ Expandable graphite/ preparation/ expansion volume分类
通用工业技术引用本文复制引用
周丹凤,田金星..低能耗型可膨胀石墨的制备研究[J].矿产综合利用,2013,(1):54-57,4.