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响应面法优化微波辅助提取五倍子单宁工艺研究

秦清 闵凡芹 徐浩 张宗和 李文君 王成章

林产化学与工业2012,Vol.32Issue(6):84-88,5.
林产化学与工业2012,Vol.32Issue(6):84-88,5.

响应面法优化微波辅助提取五倍子单宁工艺研究

Optimization of Microwave-assisted Extraction of Tannic Acid from Chinese Gallnut Using Response Surface Method

秦清 1闵凡芹 2徐浩 3张宗和 4李文君 5王成章2

作者信息

  • 1. 南京龙源天然多酚合成厂,江苏南京210032
  • 2. 中国林业科学研究院林产化学工业研究所
  • 3. 生物质化学利用国家工程实验室
  • 4. 国家林业局林产化学工程重点开放性实验室
  • 5. 江苏省生物质能源与材料重点实验室,江苏南京210042
  • 折叠

摘要

Abstract

The microwave-assisted extraction process of tannic acid from Chinese gallnut were optimized using response surface method (RSM). The effects of three independent variables, i. e. liquid to solid ratio, microwave extraction time and extraction temperature, on the yield of tannic acid, was also investigated. Results indicated that the optimum microwave-assisted extraction was obtained as the powder of Chinese gallnut 10 g, microwave power 600 W, liquid to solid ratio 32 ∶ 1 ( mL∶ g) , ultrasonic extraction time 7 min and temperature 62℃, respectively. Under this optimum condition, the extraction yield of tannic acid was 65.13%.

关键词

五倍子/单宁酸/响应面法/提取/微波

Key words

Chinese gallnut/tannic acid/response surface method/extraction/microwave

分类

化学化工

引用本文复制引用

秦清,闵凡芹,徐浩,张宗和,李文君,王成章..响应面法优化微波辅助提取五倍子单宁工艺研究[J].林产化学与工业,2012,32(6):84-88,5.

基金项目

林业公益性行业专项(201004013) (201004013)

林产化学与工业

OA北大核心CSCDCSTPCD

0253-2417

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