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溶胶-凝胶制备纳米TiO2及晶型转变的研究

尤玉飞 徐春花 王俊鹏 王镜喆 张军涛

河南科技大学学报(自然科学版)2013,Vol.34Issue(2):5-7,3.
河南科技大学学报(自然科学版)2013,Vol.34Issue(2):5-7,3.

溶胶-凝胶制备纳米TiO2及晶型转变的研究

TiO2 Nano-powders Produced by Sol-gel and Transformation of Crystal Type

尤玉飞 1徐春花 1王俊鹏 1王镜喆 1张军涛1

作者信息

  • 1. 河南科技大学材料科学与工程学院,河南洛阳471023
  • 折叠

摘要

Abstract

TiO2 nano-powders were prepared by sol-gel and were heated at 400 ~ 700 X. to study sizes and phase transformation of TiO2 nano powders. The crystalline structures and morphology of the obtained products were characterized by X-ray diffraction ( XRD ) and transmission electron microscopy ( TEM ). The relative content of various phases were analyzed by Spurr-Myers method. The results turn out that the crystalline phase transforms from anatase to rutile and the size of TiO2 nano-powders increases from 10 nm to 60 nm with increasing the temperature of heat treatment.

关键词

溶胶-凝胶法/纳米TiO2粉体/相变/温度

Key words

sol-gel/TiO2 nano-powders/phase transformation/temperature

分类

通用工业技术

引用本文复制引用

尤玉飞,徐春花,王俊鹏,王镜喆,张军涛..溶胶-凝胶制备纳米TiO2及晶型转变的研究[J].河南科技大学学报(自然科学版),2013,34(2):5-7,3.

基金项目

国家自然科学基金/香港合作基金项目(10831165504) (10831165504)

河南省教育厅自然科学基础研究计划基金项目(2010A430006) (2010A430006)

河南科技大学学报(自然科学版)

OA北大核心CSTPCD

1672-6871

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