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聚L-谷氨酸修饰电极的制备及其对扑热息痛的测定

卢先春 曹立新 孙双霞

信阳师范学院学报(自然科学版)2013,Vol.26Issue(1):115-118,4.
信阳师范学院学报(自然科学版)2013,Vol.26Issue(1):115-118,4.DOI:10.3969/j.issn.1003-0972.2013.01.027

聚L-谷氨酸修饰电极的制备及其对扑热息痛的测定

Preparation of Poly(L-Glutamic Acid)Modified Electrode and Its Analytical Application of Paracetamol

卢先春 1曹立新 2孙双霞1

作者信息

  • 1. 信阳师范学院化学化工学院,河南信阳 464000
  • 2. 河南质量工程职业学院,河南平顶山 467000
  • 折叠

摘要

Abstract

The poly ( L-glutamic acid ) modified electrode was prepared. The voltammetric behavior of paracetamol at the prepared electrode was studied. In pH 7. 0 phosphate buffer solution, the concentration of paracetamol showed good linear relationships with the oxidation peak current in the range of 0. 1 ~ 140 μmol/L with the correlation coefficients of 0.998. The limit of detection was 0.03 μmol/L (RSN =3). The developed method was used to determine paracetamol tablet samples with recoveries of 95.2% ~ 104. 8% .

关键词

聚合物修饰电极/L-谷氨酸/扑热息痛/差分脉冲伏安法

Key words

polymer modified electrode/ L-glutamic acid/ paracetamol/ differential pulse voltammograms

分类

化学化工

引用本文复制引用

卢先春,曹立新,孙双霞..聚L-谷氨酸修饰电极的制备及其对扑热息痛的测定[J].信阳师范学院学报(自然科学版),2013,26(1):115-118,4.

基金项目

河南省高校科技创新人才基金项目(2010HASTIT025) (2010HASTIT025)

信阳师范学院学报(自然科学版)

OA北大核心CSTPCD

1003-0972

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