安徽工程大学学报2012，Vol.27Issue(4)：8-11,20,5.
两步法仿生合成TiO2纳米线及其表征
Two-step synthesis of TiO2 nanowires and Characterization
摘要
Abstract
TiO2 nanowires were synthesized by using then, and L-Cys as templating agent. Solvothermal tetrabutyl titanate as titanium source was conducted synthesis of nano-TiO2 precursors was conducted. Then, nano-TiO2 precursors were treated with the hot alkaline solution at high temperatures to prepare TiO2 nanowires. Then the samples were characterized by X-ray diffraction (XRD),scanning electron microscope (SEM), FT-IR and N2 adsorption-desorption experiments. The results show that TiO2 nanowires were amorphous titanate structure, about 20;40 nm in diameter, several microns in length and the specific surface area up to 312.58 m2g. After calcining,the TiO2 nanowires changed into anatase. FT-IR spectrum analysis indicates that the samples contain Ti-O bond.关键词
TiO2/两步合成/纳米线/表征Key words
TiO2/two-step process/nanowires/characterization分类
通用工业技术引用本文复制引用
曹宁,陶玉贵,周朋,金成,孙忆晨,葛飞..两步法仿生合成TiO2纳米线及其表征[J].安徽工程大学学报,2012,27(4):8-11,20,5.基金项目
安徽省高校自然科学基金资助项目 （）
