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溶胶-凝胶法制备TiO2-C纳米复合材料的研究

邵霞 张睿 陆文聪 卢春

人工晶体学报2013,Vol.42Issue(2):305-309,315,6.
人工晶体学报2013,Vol.42Issue(2):305-309,315,6.

溶胶-凝胶法制备TiO2-C纳米复合材料的研究

Preparation of TiO2-C Nano-composite Materials by Sol-Gel Method

邵霞 1张睿 1陆文聪 1卢春1

作者信息

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摘要

Abstract

TiO2-C nanocomposite materials were prepared by using sol-gel process, which were characterized by XRD, SEM and TEM. Results showed that the precursors of TiO2 and carbon could be co-gelated soon at room temperature by adding propylene oxide as gelation initiator. TiO2 grain grows up after it is heated at 600 ℃ for 3 h, and its characteristic peak is more clear. The crystal structure of TiO2 is anatase. Ethyl acetoacetate as a complexing agent is beneficial for the formation of the gels. The pore volume and the pore diameter in the TiO2-C nanocomposite materials increase with the increasing amount of the ethyl acetoacetate.

关键词

溶胶-凝胶法/TiO2-C/纳米复合材料

Key words

sol-gel/TiO2-C/nano composite materials

分类

数理科学

引用本文复制引用

邵霞,张睿,陆文聪,卢春..溶胶-凝胶法制备TiO2-C纳米复合材料的研究[J].人工晶体学报,2013,42(2):305-309,315,6.

基金项目

上海市教委重点学科项目(J51504) (J51504)

国家自然科学基金(50872033) (50872033)

上海市科委地方高校能力建设重点项目(12160503600) (12160503600)

人工晶体学报

OA北大核心CSCDCSTPCD

1000-985X

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