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超声辅助提取华细辛挥发油中甲基丁香酚工艺优化

欧阳天贽 袁泉

天然产物研究与开发2013,Vol.25Issue(2):224-228,240,6.
天然产物研究与开发2013,Vol.25Issue(2):224-228,240,6.

超声辅助提取华细辛挥发油中甲基丁香酚工艺优化

Optimization of Extraction Process of Methyl Eugenol from Volatile Oil of Asarum Sieboldii Miq.by Ultrasound-assisted Extraction

欧阳天贽 1袁泉1

作者信息

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摘要

Abstract

In this study,the content of methyl eugenol from volatile oil of Asarum sieboldii Miq. was extracted by ultrasound-assisted extraction and determined by spiking internal standard. Based on the results of single factor experiment, orthogonal tests were designed to optimize the extraction conditions, including immersion time, material-liquid ratio, extraction temperature and time. The results showed that the best extraction conditions were as follows;3 h as immersion time, 1 : 40 as material-liquid ratio,60℃as the extraction temperature,40 min as the extraction time,with 3 parallel experimental verifications. The yields of methyl eugenol extracted out under this condition were higher than any orthogonal group. The ultrasound-assisted extraction process was proved to be stable and reliable.

关键词

华细辛/挥发油/甲基丁香酚/工艺优化/超声辅助提取

Key words

Asarum sieboldii Miq. /volatile oil/methyl eugenol/process optimization/ultrasound-assisted extraction

分类

医药卫生

引用本文复制引用

欧阳天贽,袁泉..超声辅助提取华细辛挥发油中甲基丁香酚工艺优化[J].天然产物研究与开发,2013,25(2):224-228,240,6.

基金项目

中央高校基本科研业务专项(2010-Ia-034) (2010-Ia-034)

天然产物研究与开发

OA北大核心CSCDCSTPCD

1001-6880

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