西安工程大学学报2013，Vol.27Issue(1)：79-82,4.
超声波辅助合成[Gly]Cl离子液体的研究
Study on the ultrasonic-assisted synthesis of [Gly]Cl ionic liquid
摘要
Abstract
Glycine hydrochloride ionic liquid ([Gly]Cl) was synthesized by using heating reflux and ultrasonic-assisted method. The influences of reactant molar ratio, reaction time, temperture and ultrasonic power on the yield were discussed, the enhancing effect of ultrasonic wave on the reaction was investigated. The target product was characterized by FT-IR. The optimum synthesis condition are as follows: reaction temperature, reaction time, ultrasonic power and the molar ratio of hydrochloric acid to glycine is 60℃,2h,125W and 1.8,respectively. Under the optimum condition the yield of the ionic liquid is 89.97%.关键词
甘氨酸/离子液体/超声波Key words
glycine/ionic liquid/ultrasonic分类
化学化工引用本文复制引用
肖叶群,王琛,虞登峰..超声波辅助合成[Gly]Cl离子液体的研究[J].西安工程大学学报,2013,27(1):79-82,4.基金项目
陕西省教育厅科学研究计划资助项目(12JK0465) （12JK0465）
西安工程大学博士科研启动费资助项目(DS0806) （DS0806）
