福建农林大学学报（自然科学版）2013，Vol.42Issue(2)：202-206,5.
气相色谱-质谱法测定水产品中9种合成麝香
Determination of 9 kinds of synthetic musk in aquatic products by GC-MS
摘要
Abstract
Nine kinds of synthetic musks (SMs) in aquatic products were analyzed by gas chromatography-mass spectrometry (GC-MS) and quantitated by internal standard method with ￡luoranthene-D10 after purification by florisil solid-phase extraction columns, followed by the hexane extraction for 30 minutes under ultrasonication. Under the optimized conditions, the calibration curves of all compounds were linear in the range of0.5 -100 μg · L-1 (ft2 >0.999). The limits of quantification were 0.25 -0.30 μg · L-1. The average recoveries of SM ranged from 84.1% to 116.4% with the relative standard deviations only from2.8% to9.5%. The result suggested the method was simple and accurate.关键词
合成麝香/气相色谱-质谱/水产品Key words
synthetic musk/ gas chromatography-mass spectrometry/ aquatic product分类
化学化工引用本文复制引用
叶洪,林永辉,杨方,刘正才,卢声宇,蓝锦昌..气相色谱-质谱法测定水产品中9种合成麝香[J].福建农林大学学报（自然科学版）,2013,42(2):202-206,5.基金项目
国家质检总局资助项目(2012IK033). （2012IK033）
