人工晶体学报2013,Vol.42Issue(6):1092-1097,6.
不同酸性助剂水热合成钨酸铋的制备及光催化性能研究
Preparation and Photocatalytic Activity of Bi2WO6 by Hydrothermal Method with Differrent Acid-assited
摘要
Abstract
Bi2WO6 was prepared by hydrothermal method using Bi(NO3)3 · 5H2O and Na2WO4 · 2H2Oas raw materials and NaOH as mineralizer.Samples were characterized by XRD,SEM,TEM,DRS and low-temperature N2 adsorption.Photocatalytic activity of Bi2WO6 was investigated,and the effect of Bi2WO6 by different acid-assisted hydrothermal synthesis (CH3COOH and HNO3) was also evaluated.The results reveal that acid has a significant influence on the microstructure and photocatalytic activity of Bi2WO6.HNO3 inhibits the formation of flower microspheres,makes a red shift in the absorption band and enhances the surface areas of Bi2WO6.The results of photocatalytic test reveal that HNO3 enhance photocatalytic activity of Bi2WO6,while the CH3COOH has an opposite effect.关键词
Bi2WO6/水热法/光催化活性Key words
Bi2WO6 / hydrothermal method / photocatalytic activity分类
化学化工引用本文复制引用
唐洁,展红全,江向平,徐明珠,李小红..不同酸性助剂水热合成钨酸铋的制备及光催化性能研究[J].人工晶体学报,2013,42(6):1092-1097,6.基金项目
国家自然科学基金(51262009,51062005,91022027) (51262009,51062005,91022027)
江西省自然科学基金(2010GQW0037,2010GQW0038,20114BAB216018,20122BAB202001) (2010GQW0037,2010GQW0038,20114BAB216018,20122BAB202001)
江西省主要学科学术和技术带头人培养对象计划项目(2010DD00800) (2010DD00800)
江西省高等学校"先进陶瓷材料"科技创新团队 ()
江西省教育厅项目(GJJ11204,GJJ10226,GJJ12488) (GJJ11204,GJJ10226,GJJ12488)